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panda0342
Member
- Jan 3, 2024
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Read a few other threads talking about I.V method. I know KCl is very painful and shouldn't be tried unless as a last resort. Didn't know about KNO3. You are right, it's gotta be NaNO2.The oral LD50 of potassium nitrate is between 2500 and 5000mg/kg at an average body weight in the 82kg / 180lbs range would mean oral ingestion would be in the 410g range
While SN ld50 is about 150mg/kg
Most recommend doubling the ld50 value for assurance
Which would be 820g KNO3
Vs 24.6g NaNO2
So no KNO3 would not be feasible
However high doses of KNO3 will still cause methemoglobinemia
SN can be produced through the thermal decomposition of NaNO3Read a few other threads talking about I.V method. I know KCl is very painful and shouldn't be tried unless as a last resort. Didn't know about KNO3. You are right, it's gotta be NaNO2.
Also, NaNO3 is available too. And I have easier access to KNO3 and NaNO3. Still waiting on someone to deliver some NaNO2.
Anyways, would you be so kind to tell me similar dosages for NaNO3 and KNO2?
Thanks you, PPH does recommend 25g. And a backup 25g drink, in case of vomiting.SN can be produced through the thermal decomposition of NaNO3
2NaNO3 -> 2NaNO2 + O2
61.59g of NaNO3
Starts to decompose at 380c to NaNO2
Once the reaction is complete (heating the sodium nitrate above 380) your final yeild will be about 50g of SN
The oral ld50 that I can find tested in rabbits for KNO2 is 102mg/kg at 82kg and doubling your looking at about 17g I'd still take that up to 25g as a surety following the same protocol as SN
SN can also be produced without the use of labware using NaNO3 and hydrogen peroxideThanks you, PPH does recommend 25g. And a backup 25g drink, in case of vomiting.
I don't have access to any lab equipment. Any DIY or at-home method maybe. And what about the yield's purity.
Well thanks for the efforts. But still, i don't got such equipments neither do I possess any skills in chemistry :SN can also be produced without the use of labware using NaNO3 and hydrogen peroxide
2NaNO2 + H2O2 ——> 2NaNO2 + H20 + O2
Purity in this sense is more then pure enough if anything a slight excess of peroxide to ensure full conversion maybe 10-15ml (no more then this! As to much and you can convert NaNO2 back to nitrate this can be done with standard mason jars over the counter hydrogen peroxide and sodium nitrate :)
#### Materials and Reagents:
- Sodium nitrate (NaNO3)
- 3% hydrogen peroxide (H2O2) solution
- Distilled water
- Reaction vessel (beaker or flask)
- Heat source (like a hot plate)
- Stirring rod
- Filtration setup
- Protective gear (gloves, goggles)
- Scale for measurements
#### Calculations:
1. **Required Amount of NaNO3**: Assume a 60% yield for the reaction and purification.
- Molar mass of NaNO2 = 69 g/mol
- Desired amount of NaNO2 = 50 g
- Moles of NaNO2 = 50 g / 69 g/mol ≈ 0.725 mol
- Moles of NaNO3 needed = Moles of NaNO2 (1:1 ratio) = 0.725 mol
- Molar mass of NaNO3 = 85 g/mol
- Mass of NaNO3 = 0.725 mol × 85 g/mol ≈ 61.63 g
- Adjust for 60% yield: Required NaNO3 ≈ 61.63 g / 0.60 ≈ 102.72 g
2. **Estimating Volume of 3% H2O2**:
- Assume 1 mL of 3% H2O2 per gram of NaNO3 as a starting point.
- Volume of H2O2 ≈ 102.72 mL
#### Reaction Procedure:
1. **Dissolving NaNO3**:
- Weigh out approximately 102.72 g of NaNO3.
- Dissolve NaNO3 in a minimal amount of distilled water in a reaction vessel.
2. **Adding Hydrogen Peroxide**:
- Gradually add 102.72 mL of 3% H2O2 to the NaNO3 solution while stirring continuously.
- Allow the mixture to react for several hours, occasionally stirring.
3. **Evaporation and Crystallization**:
- Gently heat the solution to evaporate excess water and hydrogen peroxide, being careful not to decompose the NaNO2.
- Allow the solution to cool slowly to room temperature, then further in a refrigerator to encourage crystallization of NaNO2.
4. **Filtration and Drying**:
- Filter the crystallized NaNO2 from the solution.
- Wash the crystals with a small amount of cold distilled water.
- Dry the sodium nitrite crystals in a desiccator or a warm, dry place.
Lol my chemistry background is showing
I'm no chemist, but the method prescribed above can definitely be done from home, where the only relatively unusual ingredient is the sodium nitrate. Luckily, you can even find these on a site as innocuous as Amazon with a high purity. If I have trouble acquiring SN from a vendor, I'll consider synthesizing it myself, tbh.Well thanks for the efforts. But still, i don't got such equipments neither do I possess any skills in chemistry :
But, if that temp method could work with stove fire, or maybe a ligher, and purity would be enough. I suppose, I could give it a try :)
I believe you zel, I guess i got scared of Materials paragraph. And sadly don't got the whole place to myself. It's a joint family system in Asia. And extraction seems like a process, that could take a day. So, I think, doable maye. Feasible, doesn't look like it :)I'm no chemist, but the method prescribed above can definitely be done from home, where the only relatively unusual ingredient is the sodium nitrate. Luckily, you can even find these on a site as innocuous as Amazon with a high purity. If I have trouble acquiring SN from a vendor, I'll consider synthesizing it myself, tbh.
Thanks @brokenpromise @zel for the confidence. Will definitely try in a three or four. I'll try to make a video, and then post it here. Much love to both of you guys <3Yah to put it in laymen's terms if you have sodium nitrate you mix the above amount with a little bit of water in a glass canning jar heck even a measuring cup add the prescribed amount of hydrogen peroxide which is found in any pharmacy pretty much in the world at 3% you wait the time I mentioned above then you bring it to a very low heat and evaporate off the liquid to be left with you SN crystal
It's actually easier then baking a cake or cookies lol
You want to use a very low heat the hydrogen peroxide in it will decompose to water and the water will evaporate off leaving you crystals
Sodium nitrate can be found most anywhere and is not regulated
I was thinking the same thing, keeping the lid off the container should evaporate water in a few hours, or maybe a day.You also don't need to heat it you could say put it in your room in a pan and just put a fan on it to remove the liquid from the crystals :) infact it can all be done in a room or bathroom or in a closet it is very very easy :)
It really makes me wonder why this isn't more well known and talked about, particularly as authorities catch on to the lethality of SN and its "associations."Yah to put it in laymen's terms if you have sodium nitrate you mix the above amount with a little bit of water in a glass canning jar heck even a measuring cup add the prescribed amount of hydrogen peroxide which is found in any pharmacy pretty much in the world at 3% you wait the time I mentioned above then you bring it to a very low heat and evaporate off the liquid to be left with you SN crystal
It's actually easier then baking a cake or cookies lol
You want to use a very low heat the hydrogen peroxide in it will decompose to water and the water will evaporate off leaving you crystals
Sodium nitrate can be found most anywhere and is not regulated
You absolutely should! I think that we as a community should try to help and inform each other as much as possible about alternative means to the same desired result: safe and reliable options for CTB (so that they can make an informed choice). With all the unceasing and ubiquitous demands for the PMing of sources, I think this may be something we can get behind :) Best of luckThanks @brokenpromise @zel for the confidence. Will definitely try in a three or four. I'll try to make a video, and then post it here. Much love to both of you guys <3
2NaNO2 + H2O2 ——> 2NaNO2 + H20 + O2
Honestly I'm not to sure to be fair I think a lot of people with depression and low self confidence who want to CTB aren't typically going to take the time to synthesize SN as Even if CTB is planned out the final act is often impulsive and convenient.It really makes me wonder why this isn't more well known and talked about, particularly as authorities catch on to the lethality of SN and its "associations."
I have to ask: If all this can be done with next to no formal chemistry background and the ingredients are readily available (less than $20 online, let's say), why are so many so skeptical of it? Is it because the notion of creating it yourself is intimidating - people are afraid of ending up with an impure product? Speaking of, how would you go about ensuring that the end product is thoroughly transmuted and consequently fit for CTB?
You are absolutely correct I mistyped I will correct thatYou absolutely should! I think that we as a community should try to help and inform each other as much as possible about alternative means to the same desired result: safe and reliable options for CTB (so that they can make an informed choice). With all the unceasing and ubiquitous demands for the PMing of sources, I think this may be something we can get behind :) Best of luck
I will also post my progress and results in this method when I begin!
You mean 2NaNO3 + H202 —> , right?
Also, you (naturally) mention that the sodium nitrate will need to be dissolved in distilled water, but you mention it being a "minimal" level; does that mean it does not need to be fully saturated/dissolved in the solution? If not, why is that?
Thanks!
Add KNO2 is also good for CTB? Like It would be, as effective as NaNO2 and what about side effects and dosage. Because, Potassium Nitrate is readily available to everyone, as a fertilizer everywhere.Oh also you can do the same for potassium nitrate
Approximately 59.41g of KNO3.
Between 22 mL to 24 mL of 3% H2O2 (considering a 10-20% excess).
To yield KNO2 :)
Fertilizer grade nitrate will contain binders see my above mention near the bottom about removing said binders in my last postAdd KNO2 is also good for CTB? Like It would be, as effective as NaNO2 and what about side effects and dosage. Because, Potassium Nitrate is readily available to everyone, as a fertilizer everywhere.
Yeah, It is my first day here on SS. And I have seen tons of confusing posts. Will update this thread, once I synthesize, but gonna wait for @brokenpromise experiment. I think, he/she is a professional. And after his success. If I could get it to work. Than most definitely anyone can.You absolutely should! I think that we as a community should try to help and inform each other as much as possible about alternative means to the same desired result: safe and reliable options for CTB (so that they can make an informed choice). With all the unceasing and ubiquitous demands for the PMing of sources, I think this may be something we can get behind :) Best of luck
I will also post my progress and results in this method when I begin!
I just wish, I could kiss your hands right now. Here I was tired & distressed, been reading everything from the past 2 months. I tried, Google, Bing, DuckDuckGo, Yandex. Every resource i could find. And Wham, you gave me the clarity I needed. No other resource mentions KNO2's lethality, nor for any other compound.Fertilizer grade nitrate will contain binders see my above mention near the bottom about removing said binders in my last post
The oral LD50 of potassium nitrite is about 200mg per kg so at 82kg body mass would be 16.4g x2 to ensure effective dosing I would say 32.8g of kno2 would be lethal
Following the same protocol as SN and having 2 glasses of 32.8g each of kno2 solution
Thanks for theYeah, It is my first day here on SS. And I have seen tons of confusing posts. Will update this thread, once I synthesize, but gonna wait for @brokenpromise experiment. I think, he/she is a professional. And after his success. If I could get it to work. Than most definitely anyone can.
I just wish, I could kiss your hands right now. Here I was tired & distressed, been reading everything from the past 2 months. I tried, Google, Bing, DuckDuckGo, Yandex. Every resource i could find. And Wham, you gave me the clarity I needed. No other resource mentions KNO2's lethality, nor for any other compound.
If you have seen Marvel's Thor Ragnarok. Consider yourself Loki
lol thanks for the vote of confidence hahaYeah, It is my first day here on SS. And I have seen tons of confusing posts. Will update this thread, once I synthesize, but gonna wait for @brokenpromise experiment. I think, he/she is a professional. And after his success. If I could get it to work. Than most definitely anyone can.
I just wish, I could kiss your hands right now. Here I was tired & distressed, been reading everything from the past 2 months. I tried, Google, Bing, DuckDuckGo, Yandex. Every resource i could find. And Wham, you gave me the clarity I needed. No other resource mentions KNO2's lethality, nor for any other compound.
If you have seen Marvel's Thor Ragnarok. Consider yourself Loki
He's the expert here - though I am happy to help with any medically related questions, being in that field - so take this with a grain of salt (no pun intended): It seems that according to some sources I was able to dig up, the LD50 of the potassium nitrite is 235mg/kg, rather than 200mg/kg. So if you want to be a real stickler about it, I'd warn that this may be a YMMG situation and err on going on the upper end of your intended dosage.Yeah, It is my first day here on SS. And I have seen tons of confusing posts. Will update this thread, once I synthesize, but gonna wait for @brokenpromise experiment. I think, he/she is a professional. And after his success. If I could get it to work. Than most definitely anyone can.
I just wish, I could kiss your hands right now. Here I was tired & distressed, been reading everything from the past 2 months. I tried, Google, Bing, DuckDuckGo, Yandex. Every resource i could find. And Wham, you gave me the clarity I needed. No other resource mentions KNO2's lethality, nor for any other compound.
If you have seen Marvel's Thor Ragnarok. Consider yourself Loki
@zel @brokenpromise I am a Software Engineer. And If you need any help with researching, testing or anything related to our community. Let me know, I'd like to take some some things on for SS.
Thanks for that I agree there can be a bit of conflictinon in the LD50 both on sources and also on animal rat vs rabbitHe's the expert here - though I am happy to help with any medically related questions, being in that field - so take this with a grain of salt (no pun intended): It seems that according to some sources I was able to dig up, the LD50 of the potassium nitrite is 235mg/kg, rather than 200mg/kg. So if you want to be a real stickler about it, I'd warn that this may be a YMMG situation and err on going on the upper end of your intended dosage.
I've also heard murmurs about KN being slightly more caustic/painful than SN? This may be nothing but misinformation though, and I cannot confirm that this is any more than the unwarranted speculation of randos. What I can say is that the mechanism of action in both cases (hypoxia secondary to methemeglobinemia) is absolutely the same, and that the KN is only marginally less toxic. As such, my working hypothesis is that there is little to no difference in the effect on the body (both nitrites after all), and unless there is some digestive irritation, the process would be just as smooth.
You know one thing I have been considering is a ardunio or similar ble interface to a pulse oximeter somthing like a BM1000 that could poll for data ever 30 seconds to record heart rate and SpO2 maybe a nodemcu with ble support that could host a captive portal for wifi login then it would push the readings to a site with a given username and allow people through the portal to document their ctb attempt with time stamps if they want this would not only give affirmative confirmation to the community on ctb but also provide real life data as to effectiveness of certain methods etcYeah, It is my first day here on SS. And I have seen tons of confusing posts. Will update this thread, once I synthesize, but gonna wait for @brokenpromise experiment. I think, he/she is a professional. And after his success. If I could get it to work. Than most definitely anyone can.
I just wish, I could kiss your hands right now. Here I was tired & distressed, been reading everything from the past 2 months. I tried, Google, Bing, DuckDuckGo, Yandex. Every resource i could find. And Wham, you gave me the clarity I needed. No other resource mentions KNO2's lethality, nor for any other compound.
If you have seen Marvel's Thor Ragnarok. Consider yourself Loki
@zel @brokenpromise I am a Software Engineer. And If you need any help with researching, testing or anything related to our community. Let me know, I'd like to take some some things on for SS.
Where did you find out about that reaction, dear alchemist? It's not even balanced correctly, since you have 8 atoms of oxygen on the left side and only 7 atoms of oxygen on the right side.SN can also be produced without the use of labware using NaNO3 and hydrogen peroxide
2NaNO3 + H2O2 ——> 2NaNO2 + H20 + O2
3% (mass) from 102.72 mL of H2O2 solution is nearly 3 g or 0.1 mol of H2O2.#### Calculations:
1. **Required Amount of NaNO3**: Assume a 60% yield for the reaction and purification.
- Molar mass of NaNO2 = 69 g/mol
- Desired amount of NaNO2 = 50 g
- Moles of NaNO2 = 50 g / 69 g/mol ≈ 0.725 mol
- Moles of NaNO3 needed = Moles of NaNO2 (1:1 ratio) = 0.725 mol
- Molar mass of NaNO3 = 85 g/mol
- Mass of NaNO3 = 0.725 mol × 85 g/mol ≈ 61.63 g
- Adjust for 60% yield: Required NaNO3 ≈ 61.63 g / 0.60 ≈ 102.72 g
2. **Estimating Volume of 3% H2O2**:
- Assume 1 mL of 3% H2O2 per gram of NaNO3 as a starting point.
- Volume of H2O2 ≈ 102.72 mL
That looks like alchemy background, LMAO.Lol my chemistry background is showing
Don't worry, that's just a joke.It really makes me wonder why this isn't more well known and talked about, particularly as authorities catch on to the lethality of SN and its "associations."
I have to ask: If all this can be done with next to no formal chemistry background and the ingredients are readily available (less than $20 online, let's say), why are so many so skeptical of it?
Do u know What is the shelf life of SN in a closed plastic bottle and also if the bottle is left open? A way to test purity of sn?Yah to put it in laymen's terms if you have sodium nitrate you mix the above amount with a little bit of water in a glass canning jar heck even a measuring cup add the prescribed amount of hydrogen peroxide which is found in any pharmacy pretty much in the world at 3% you wait the time I mentioned above then you bring it to a very low heat and evaporate off the liquid to be left with you SN crystal
It's actually easier then baking a cake or cookies lol
You want to use a very low heat the hydrogen peroxide in it will decompose to water and the water will evaporate off leaving you crystals
Sodium nitrate can be found most anywhere and is not regulated
Good point, I missed that while reading. Is there any particular reason it couldn't be rewritten as one molecule of each? I.e. NaNO3 + H202 —> NaNO2 + H20 + O2Where did you find out about that reaction, dear alchemist? It's not even balanced correctly, since you have 8 atoms of oxygen on the left side and only 7 atoms of oxygen on the right side.
you are correct it is balancedGood point, I missed that while reading. Is there any particular reason it couldn't be rewritten as one molecule of each? I.e. NaNO3 + H202 —> NaNO2 + H20 + O2
I'm pretty sure that's balanced, but there may be some simple reason why it must be 2NaNO3 and 2NaNO2 that I'm unaware of, since I have little chemistry background.
Heart rate would be a good indicator of the body's early response and detection of hypoxia. Using an ECG would be a strict upgrade diagnostically, though. It would allow for precise documentation of the onset of Vtach and of (more importantly) Vfib.You know one thing I have been considering is a ardunio or similar ble interface to a pulse oximeter somthing like a BM1000 that could poll for data ever 30 seconds to record heart rate and SpO2 maybe a nodemcu with ble support that could host a captive portal for wifi login then it would push the readings to a site with a given username and allow people through the portal to document their ctb attempt with time stamps if they want this would not only give affirmative confirmation to the community on ctb but also provide real life data as to effectiveness of certain methods etc
What's your thoughts ? I was more so thinking of outsourcing it to a 3rd party developer in like India as I'm mostly a script kiddy who can just barely hack his way around code there is admittedly a morbid curiosity within me that also is rooted in scientific data
No problem! I have confidence we'll get something figured out :)Yes
you are correct it is balanced
But the redox reaction is not necessarily going to yield the desired result
The other possibility is yielding NaO and HNO3
2 NaNO3 + H2O2 = 2 NaO + 2 HNO3
Though I would say is less likely
Im big enough man to realized I had make a prior mistake it happens this is why we run tests and experiments and im working on it.
Im doing a practical experiment now in real life and i will report on the results when possible
And when i get home this evening i will review all my procedures / math and verify / correct everything to ensure everything is factual and up to date my apologies for the prior misinformation I was doing math in my head and on my phone rather then on pen and paper and typing it out properly